Sunday 8 June 2014

Vickers hardness

Hardness is the property of a material that enables it to resist plastic deformation, usually by penetration. However, the term hardness may also refer to resistance to bending, scratching, abrasion or cutting.
The Vickers hardness test was developed in 1921 by Robert L. Smith and George E. Sandland at Vickers Ltd as an alternative to the Brinell method to measure the hardness of materials.[1] The Vickers test is often easier to use than other hardness tests since the required calculations are independent of the size of the indenter, and the indenter can be used for all materials irrespective of hardness. The basic principle, as with all common measures of hardness, is to observe the questioned material's ability to resist plastic deformation from a standard source. The Vickers test can be used for all metals and has one of the widest scales among hardness tests. The unit of hardness given by the test is known as the Vickers Pyramid Number (HV) or Diamond Pyramid Hardness (DPH). The hardness number can be converted into units of Pascal’s, but should not be confused with a pressure, which also has units of Pascal’s. The hardness number is determined by the load over the surface area of the indentation and not the area normal to the force, and is therefore not a pressure.[1]
It is the standard method for measuring the hardness of metals, particularly those with extremely hard surfaces: the surface is subjected to a standard pressure for a standard length of time by means of a pyramid-shaped diamond. The diagonal of the resulting indention is measured under a microscope and the Vickers Hardness value read from a conversion table. 
Vickers hardness is a measure of the hardness of a material, calculated from the size of an impression produced under load by a pyramid-shaped diamond indenter. 

A method of determining the hardness of steel whereby a diamond pyramid is pressed into the polished surface of the specimen and the diagonals of the impression are measured with a microscope fitted with micrometer eye piece. The rate of application and duration are automatically controlled and the load can be varied. Two types of indenters are generally used for the Vickers test family, a square base pyramid shaped diamond for testing in a Vickers hardness tester and a narrow rhombus shaped indenter for a Knoop hardness test
 
2.  WORKING PRINCIPLE
The Vickers hardness test method consists of indenting the test material with a diamond indenter, in the form of a right pyramid with a square base and an angle of 136 degrees between opposite faces subjected to a load of 1 to 100 kg. The full load is normally applied for 10 to 15 seconds. The two diagonals of the indentation left in the surface of the material after removal of the load are measured using a microscope and their average calculated. The area of the sloping surface of the indentation is calculated. The Vickers hardness is the quotient obtained by dividing the kgf load by the square mm area of indentation
 

The Vickers hardness test operates on similar principles to the Brinell test, the major difference being the use of a square based pyramidal diamond indenter rather than a hardened steel ball. Also, unlike the Brinell test, the depth of the impression does not affect the accuracy of the reading so the P/D2 ratio is not important. The diamond does not deform at high loads so the results on very hard materials are more reliable. The load may range from 1 to 120kgf and is applied for between 10 and 15 seconds.         
As illustrated in the figure, two diagonals, d1 and d2, are measured, averaged and the surface area calculated then divided into the load applied. As the hardness may be reported as Vickers Hardness number (VHN), Diamond Pyramid Number (DPN) or, most commonly, Hv xx where 'xx' represents the load used during the test [2].

F= Load in kgf.
d = Arithmetic mean of the two diagonals, d1 and d2 in mm
HV = Vickers hardness
Vickers Scale Formula
The Vickers hardness number, reported as HV, is the ratio of the force applied to the indenter (kgf) to the surface area (mm²) of the indentation. When the mean diagonal of the indentation has been determined the Vickers hardness may be calculated from the formula, but is more convenient to use conversion tables. The Vickers hardness should be reported like 800 HV/10, which means a Vickers hardness of 800, was obtained using a 10 kg force. Several different loading settings give practically identical hardness numbers on uniform material, which is much better than the arbitrary changing of scale with the other hardness testing methods. The advantages of the Vickers hardness test are that extremely accurate readings can be taken, and just one type of indenter is used for all types of metals and surface treatments. Although thoroughly adaptable and very precise for testing the softest and hardest of materials, under varying loads, the Vickers machine is a floor standing unit that is more expensive than the Brinell or Rockwell machines.
 There is now a trend towards reporting Vickers hardness in SI units (MPa or GPA) particularly in academic papers. Unfortunately, this can cause confusion. Vickers (e.g. HV/30) value should normally be expressed as a number only (without the unit’s kgf/mm2). Rigorous application of SI is a problem. Most Vickers hardness testing machines use forces of 1, 2, 5, 10, 30, 50 and 100 kgf and tables for calculating HV. SI would involve reporting force in Newton’s (compare 700 HV/30 to HV/294 N = 6.87 GPa) which is practically meaningless and messy to engineers and technicians. To convert Vickers hardness number the force applied needs converting from kgf to Newton’s and the area needs converting form mm2to m2 to give results in Pascal’s using the formula above [2].
 To convert HV to MPa multiply by 9.807

To convert HV to GPA multiply by 0.009807

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